It's Tingle Time! - Marvel Team-Up #13 (1973)

Peter is in San Francisco and still a little messed up about Gwen's death. To help cheer himself up, he goes looking for crime and finds it not long later when he runs into some AIM beekeepers. After following the trail he runs into Captain America and together they try to stop the Grey Gargoyle from launching a satellite to space that will unless a ray that will turn anyone he wants into stone. Will the wall crawler and the sentinel of liberty be able to stop him?